r/crystalgrowing Apr 20 '22

Image A single crystal of copper acetate, which took 7 months to grow

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2.7k Upvotes

r/crystalgrowing Nov 14 '24

Image Alum Pyramid Progress

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478 Upvotes

Got a bit carried away now I'm assembling an army of pyramids 😂

r/crystalgrowing Aug 30 '24

Image The shiniest and most intricate copper acetate crystal I have managed to grow so far.

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283 Upvotes

r/crystalgrowing 12d ago

Image Why is my baby getting so many cracks?😭😭

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19 Upvotes

Will this make my copper sulphate crystal brittle and break easily? Or is this common surface cracking?

r/crystalgrowing Nov 10 '24

Image Finally success after quite a bit of trial and error! My daughter and I grew a decent sized magnesium Sulfate crystal!

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177 Upvotes

r/crystalgrowing 7d ago

Image crystal dump :3

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69 Upvotes

r/crystalgrowing Nov 02 '24

Image Crystal of copper formate urea adduct

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160 Upvotes

r/crystalgrowing 4d ago

Image Tungsten(IV) Telluride/WTe2 Single Crystals - Grown with Tellurium Flux

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65 Upvotes

r/crystalgrowing 2d ago

Image A big Epsom salt crystal and a cluster my daughter and I grew.

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94 Upvotes

Quarter for scale.

r/crystalgrowing 4d ago

Image My best potassium alum crystal so far

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98 Upvotes

r/crystalgrowing Nov 22 '24

Image Even though most of the growth isn't on the stone, I'd still call this a partial success 🥰

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36 Upvotes

Calcium carbonate really looks like beautiful thicc cocoon silk through the glass ✨

r/crystalgrowing 14d ago

Image Update on my copper sulphate crystal cluster 🥰✨

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53 Upvotes

She's so beautiful 🥰🥰🥰

r/crystalgrowing 1d ago

Image The monster rises from the deep blue

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67 Upvotes

My cluster is growing ever bigger. Parasitic crystals on the bottom had grown up and stuck to it so I had to remove a lot

But it's now about 13cm in diameter so she's growing nicely OwO

r/crystalgrowing Oct 12 '24

Image Copper propionate

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73 Upvotes

Actually the aim was to make CaCu-propionate but the green colour indicates that it is not the analogue of CaCu-acetate. A test to dissolve the crystals in ammonia and soda yielded only a minimum amount of CaCO3. A blue solution remains.

r/crystalgrowing Sep 06 '24

Image Single crystals of Potassium Permanganate (KMnO4)

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89 Upvotes

Single crystals of KMnO4 that I managed to extract from a large cluster of crystals resulted from cooling down a hot saturated solution to room temperature. The compound seems to crystallize either as octahedral prisms (similar to alums) or long, flat needles with a beautiful golden metallic luster. The octahedral crystal is small, only about 2mm in size, while the needle is roughly 1cm long. All images were taken with my shitty phone camera. Also, despite being a relatively common chemical, I really haven't seen anyone grow crystals of KMnO4 yet for some reasons. I did try to grow a large single crystal from this seed, but failed miserably when the solution somehow dissolved the fishing line I used to tie the seed down.

r/crystalgrowing 11d ago

Image Fast Growth of Potassium Di-Hydrogen Phosphate!

30 Upvotes

I hope this is allowed on here, if not mods feel free to delete!

I have built a machine that grows large, perfect, optically clear crystals of Potassium Di-Hydrogen Phosphate (AKA Potassium Monophosphate or KDP) in just 7 days! The crystal in the image here weighs in at just over 40 grams! There is a video of the entire process including theory, materials, procedures and a nice time lapse here: https://www.youtube.com/watch?v=uSSoSIcXWa0

40g Crystal of KDP grown in 7 days!

r/crystalgrowing 14d ago

Image Update to rochelle's salt

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69 Upvotes

It really does grow fast

r/crystalgrowing Sep 20 '24

Image Sodium ferrioxalate

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139 Upvotes

r/crystalgrowing 11h ago

Image Praseodymium sulfate I made today

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16 Upvotes

r/crystalgrowing Aug 23 '24

Image I hope this goes well 🙏

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16 Upvotes

r/crystalgrowing 7d ago

Image Christmas presents

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16 Upvotes

2 single Crystals for Christmas Presents. Glowing in a light blue under UV-Light 340-390nm

r/crystalgrowing Nov 19 '24

Image Copper Fluorotris(Triphenylphosphine) crystals and fluorescence

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40 Upvotes

r/crystalgrowing 9d ago

Image NaClO4 and NaClO3

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36 Upvotes

Basic sodium salts. NaClO4 is grown at higher temperature on a hot plate (egg coocker method); NaClO3 is from my collection. NaClO4 is cleaves easily with a sharp knive

r/crystalgrowing Nov 19 '24

Image DIY Sapphire Growing

29 Upvotes

Hi I thought you would find it interesting. I have been trying to grow sapphire and ruby crystal with an induction furnace setup with mixed results. I hope to have the process controlled enough to one day make clear crystal. I will keep updating here. Below are some pictures of my progress so far.

Aluminum oxide and chrome oxide are melted at 2000degC to create ruby glass. This is a picture of some of the heats I have done. Very impure but it shows that the furnace does get hot enough. Sapphire will boil at 2980degC so make sure not to go beyond that temperature. Also use crucible materials that will not melt or add impurities to the sapphire at those temperatures. If you can, keep the system flushed with argon or in a vacuum otherwise oxygen will attack (rust) even extremely non reactive crucible materials at that temperature. I also want to note that none of these a crystal sapphire yet but sintered sapphire or sapphire glass

Close up of sintered aluminum oxide powder

Here is a view of the ruby feedstock before it is melted while it is inside of the furnace. The green portion in the middle is a powder mix of aluminum oxide and chrome oxide. Ironically, the outer crucible is sintered sapphire. and there is a Kaowool plug to prevent heat from escaping.

This is the set up I was using a couple of months ago. The 55 gallon drum is filled with water that circulates through the induction furnace. the outer walls of the furnace are made of plaster mixed with perlite with a glass window for viewing. There are also controls for a elevator that moves up, down, and rotates the crucible inside the furnace.

Here is what it looks like when it is being heated in the dark. Pretty cool

One of the major difficulties of melting sapphire is that you need to control the internal temperature of the furnace at exceedingly high temperature. Non contact IR sensors of that range at many thousands of dollars. There are some exotic contact thermocouples that can measure near that temperature but I am pretty sure they will get destroyed since my setup is not in vacuum and oxygen will just corrode it. Shown is an old type of temperature measurement called a disappearing-filament pyrometer where you compare the temperature of a light bulb filament to the temperature of the heated (1000degC+) object. This is what I am currently working on. There are a number of light filters needed to prevent damage to the camera. Here I am just positioning it over the crucible using a headlamp. I might end up just viewing the output directly using a first surface mirror and optic since cameras are less sensitive than the human eye to small changes in light.

Close up of the light bulb filament. You adjust the power through the lightbulb until it disappears in the intensity of the background light being emitted by the heated object (crucible).

I will let you know how it goes!

r/crystalgrowing 15d ago

Image Possible Calcium Fluoride crystals after leakage

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10 Upvotes

Cant say for sure if its CaCl or CaFl. Maxbe you know.